Reference Material 8457 is intended to help address concerns about the long-term durability of orthopedic hip implants amid growing use of these devices in younger, more active patients. It is well known that radiation can create new chemical bonds between adjacent molecular chains in a special form of polyethylene used to make the socket for the metal ball and shaft in an artificial hip. This "crosslinking" creates a structure that resists sliding forces and wear. Manufacturers and researchers need to control radiation conditions to achieve the intended wear resistance; too much radiation causes brittleness, and too little can result in poor wear resistance.
The NIST material consists of 10 small, identical cubes of polyethylene. The cubes are intended for use as control samples in a new ASTM International standard test method. The method involves immersing cubes in an organic liquid and measuring how much the material swells. Samples that expand the most have the least amount of crosslinking. Each reference material comes with a certificate that provides precise cube dimensions and information about swelling from a series of round-robin tests involving six laboratories.
The reference material will help researchers and implant manufacturers control or optimize a variety of processing parameters, such as the type (gamma radiation or electron beams), timing, and doses of radiation used for crosslinking.